I would imagine this has been covered here before, but I didn't find it via the search function. Oh well.
It's pretty basic:
-- Make sure your drive is down in the "run" or "trim" position, not the "tilt" range (you should know all about the difference, now - based on your other post :smt001)
-- Attach muffs with a good water supply. Water will be squirting out quite forcefully from around the muffs.
-- Start the engine. Check to see that the muffs stay attached as sometimes it can slide off.
-- The "better" muffs (as mentioned above) will actually have a small rod that goes through the water inlet. It prevents the muff from sliding off by connecting the two halves of the muff together.
-- Not necessary, but I also make it a habit to see that I have exhaust water exiting through the bottom of the transom plate. (3.0L 4cyls will only exit on one side). To see what I mean, feel around the bottom of the transom plate - you'll find two holes that you can stick your fingers in.